Suomen ympäristökeskus

This document specifies methods for the measurements of magnetic susceptibility of soils (?) as an indicator of potential soil pollution/contamination with trace elements associated with technogenic magnetic particles (TMPs) and describes related procedures, protocols and guidelines to be applied as a screening geophysical method of determination of soil pollution with trace elements. The results of measurements are used for preparing the maps of magnetic susceptibility of soils in the area of interest. From these maps, the areas of elevated and high magnetic susceptibility indicating high trace element total pollution load are discriminated for further identification of pollutants by geochemical methods. This document is applicable to screening all TMPs-related anthropogenic emission sources including long-range transport of airborne elements, of which TMPs are carriers and indicators. Such emission sources comprise the majority of high-temperature industrial processes, where iron is present in any mineralogical form in raw materials, additives or fuels, is transformed into ferrimagnetic iron oxides (e.g. fossil solid and liquid fuels combustion, metallurgy, cement and ceramics industry, coke production, industrial waste landfills, land transport). This document is not applicable to screening anthropogenic emissions not associated with TMPs, e.g. organic pollutants or emissions from agricultural sources. In rare cases, some soils are developed on bedrock exhibiting geogenically high magnetism, which can cause false-positive results. This influence can, however, be easily indicated by measurements of magnetic susceptibility along soil profiles. This method is not applicable when the bedrock exhibits extremely high magnetic signals.

This procedure specifies a method for the determination of 228Ra activity in drinking waters by radiumextraction, purification and liquid scintillation counting.

This document specifies three methods for the digestion of soil, treated biowaste, sludge and waste by the use of an acid mixture composed of hydrochloric (HCl), nitric (HNO3) and tetrafluoroboric (HBF4) or hydrochloric (HCl), nitric (HNO3) and hydrofluoric (HF) acid as the digestion solution.Digestion with these acids is effectively considered as a total decomposition of the sample. For a broad range of samples the extracted analyte concentrations will reflect the total content in the sample.This document is applicable for the following elements:Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), nickel (Ni), phosphorus (P), potassium (K), selenium (Se), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tellurium (Te), thallium (Tl), tin (Sn), titanium (Ti), vanadium (V), and zinc (Zn).This document can also be applied for the digestion of other elements, provided the user has verified the applicability.

This standard specifies a method for the measurement of iron-55 and nickel-63 (55Fe and 63Ni)in all types of waters by liquid scintillation counting (LSC).The detection limit depends on the sample volume and the instrument used. The test method described in this standard is based on currently available LSC counters.

This document specifies a method for the determination of total dissolved solids (TDS) in water and eluates, provided they are not volatile under the conditions specified or that they do not release water molecules from hydration. It applies to water and eluates containing more than 100 mg/l of total dissolved solids. Samples with lower amounts of dissolved solids can be analysed by repetition of the drying step.